Pharmaceutical Inorganic Chemistry Practical

Aim: To perform the limit test for heavy metals for the given sample. Requirements: Nessler cylinders, 1ml bulb pipette, dilute acetic acid, dilute ammonia solution, hydrogen sulphide solution, pH paper: 3-4 range, lead standard solution (20 ppm Pb), glass rods. Principle: In this experiment, the test color obtained by the reaction of heavy metal impurities …

Aim: To perform the limit test for iron for the given sample. Requirements: Nessler cylinder, 2ml bulb pipette, 20% w/v iron-free citric acid, thioglycolic acid, ammonia solution, iron standard solution (20 ppm Fe), glass rods, red-litmus paper. Principle: In this experiment, the test color (purple) obtained by the reaction of iron impurities with mercaptoacetic acid …

Aim: To perform limit test for sulphates for the given sample. Requirements: Nessler cylinders, glass rod, 1ml bulb pipette, 2 ml graduate pipette, 5 M acetic acid, sulphate standard solution (10 ppm SO4), test sample, barium chloride solution, ethanolic sulphate standard solution (10 ppm SO4), 1ml graduate pipette. Principle: In this experiment, the test opalescence/turbidity …

Aim: To perform limit test for chlorides for the given sample. Requirements: Nessler cylinders, glass rod, measuring cylinders, 1ml bulb pipette, 10 ml bulb pipette, dilute nitric acid, 0.1 M silver nitrate, chloride standard solution (25 ppm Cl), test sample. Principle: In this experiment, the test opalescence obtained by the reaction of chloride impurities with …

Cerimetry or cerimetric titration, also known as cerateoximetry.It is a redox titration in which a Fe2+-1,10-phenanthroline complex (ferroin) color change indicates the endpoint. (Ferroin) can be reversibly discolored in its oxidized form upon titration with a Ce4+ solution. Standard solutions can be prepared from different Ce4+ salts, but often cerium sulfate is chosen. Procedure: Since …